The effect of hydrofluoric acid treatment on the repair strength of polyamide denture base materials: An in vitro study

Abstract

Purpose: Although polymethylmethacrylate (PMMA) dentures can be repaired using autopolymerizing acrylic resin, achieving it using polyamides is difficult. This study aimed to achieve acceptable bond strength using autopolymerizing acrylic resin by applying surface treatments to the polyamide denture base material.

Materials and methods: Thirty-six disc-shaped samples (27 polyamide, 9 PMMA) were prepared. Based on the surface treatment applied, the polyamide samples were divided into three groups: No surface treatment (n = 9), tribochemical silica coating + silane coupling agent (n = 9), and 9% hydrofluoric acid + tribochemical silica coating +silane coupling agent (n = 9). PMMA specimens received no surface treatment. Polyamide and PMMA surfaces had auto-polymerizing acrylic resin bonded on them, and then a shear bond strength test was performed between them after aging. The Kruskal-Wallis test was used, and statistical significance was set at p < 0.05.

Results: PMMA had the highest shear bond strength, the untreated polyamide group had the lowest shear bond strength, and the difference was significant (p < 0.05). The group treated with 9% hydrofluoric acid, tribochemical silica coating, and silane coupling agent exhibited the highest shear bond strength of the polyamide groups, and the bond strength in this group was comparable to the PMMA specimens (p > 0.05).

Conclusions: The polyamide denture repair strength can be improved by 9% hydrofluoric acid, tribochemical silica coating, and silane coupling agent application to the polyamide surface.